Practical Manual of Analytical Chemistry

Practical manual of analytical chemistry is written with the idea of presenting a well-documented, student friendly laboratory manual for B.Pharmacy 1st year students. It is being observed during academic experience that students have problems in understanding the basic concepts and the calculation part. Most of the students generally transfer the instructions to practical book without clearing the basic concept. Practical manual has been revised according to the latest syllabus as prescribed by Pharmacy Council of India. Hope this manual will meet the needs and requirements of undergraduate pharmacy students.
Contents:

LIMIT TEST
1. To perform the limit test for chlorides in the given sample of Sodium Chloride (NaCl)
2. To perform the limit test for sulphate in the given sample of Potassium Sulphate (K2SO4)
3. To perform the limit test for iron in the given sample of Sodium Chloride (NaCl)
4. To perform the limit test for arsenic in the given sample of Magnesium Sulphate (MgSO4)
5. To Prepare and standardize 250 ml of approximately 0.1N Sodium Hydroxide (NaOH)
6. To Prepare and standardize 250 ml of approximately 0.1N Sulphuric acid (H2SO4)
7. To Prepare and standardize 250 ml of approximately 0.1M Sodium thiosulphate (Na2S2O3)
8. To prepare and standardize 250 ml of approximately 0.1 N Potassium permanganate (KMNO4)
9. To prepare and standardize 250 ml of approximately 0.1 N Ceric Ammonium Sulphate (NH4Ce (SO4)4) 2H2O
10. To determine the % age purity of given sample of Ammonium Chloride.
11. To find out the percentage purity of given sample of Ferrous Sulphate (FeSO4.7H2O)
12. To determine the percentage purity of given sample of Copper Sulphate (CuSO4.5H2O)
13. To find out the % age purity of given sample of Calcium Gluconate
14. To determine the % age purity of given sample of Hydrogen Peroxide (H2O2).
15. To determine the % age purity of given sample of Sodium

Benzoate
16. To determine the % age purity of given sample of Sodium chloride. ELECTRO ANALYTICAL METHODS
17. To determine the normality of strong acid (H2SO4) in the given unknown solution by titrating against strong base (NaOH) using conductometry.
18. To determine the normality of strong acid (H2SO4) and weak acid (CH3COOH) in the given unknown solution by titrating against strong base (NaOH) using conductometry
19. To determine the normality of strong acid (H2SO4) in the given unknown solution by titrating against strong base (NaOH) potentiometrically.

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